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Magnetic Force Microscopy

Magnetic force microscopy (MFM), is a family of techniques used to measure magnetic fields using an AFM. In fact there are a large number of different  techniques used to measure magnetic properties, but in general, they all use the AFM to measure the oscillation of a magnetically sensitive probe when it is far (5-100 nm) from the sample surface. MFM probes are usually made by coating normal silicon probes with a thin magnetic coating. The magnetic coating means that the oscillation of the probe will change when in a magnetic field. However, when the probe is touching the sample, the short range tip-sample forces will obscure the magnetic forces (which are much weaker). Fortunately, since magnetic forces can be measured at a distance, it is possible to remove the probe from the surface, and still measure magnetic forces, while removing these short range forces. In order to make accurate measurements, the probe should be at the same distance from the sample throughout the image. There are a number of techniques to do this, which are reviewed in [1], but in most commercial implementations, the so-called “Lifting” method first used by Bard [2] is used. This method is illustrated schematically below.

 

How MFM lifting modes work

In order to make MFM measurements with this lifting mode, an oscillating mode is used, typically intermittent contact mode AFM. For each line of the image, two scans are made. In the first line, the topography is measured as usual. The probe is then lifted a user-defined distance above the surface (typically in the range 5 to 50 nm). The second line will then be measured, but the topography measured in the first line is added to the height of the probe as it scans along the line. In this way, the instrument attempts to keep the probe at exactly the same distance from the sample surface at each point in the MFM image. MFM is widely used to generate images of magnetic fields associated with small domains, and is particularly of use in the development of magnetic recording technology . It can also show magnetic fields associated with individual magnetic nanoparticles[3]. However, interpretation of MFM signals is complicated by the unknown nature of the probe, and it is limited to measuring fairly intense fields[4,1].

mfm

The image above shows topogrpahic (left) and magnetic field (right) images of a cluster of magnetic nanoparticles.

 

References

Eaton P et al. (2010) Atomic force microscopy. OUP, Oxford

Lin CW et al. (1987). J Electrochem Soc 134:1038-1039.

 Neves CS et al. (2010). Nanotechnology 21:305706.

Schreiber S et al. (2008). Small 4:270-278.


book coverThis article was condensed from “Atomic Force Microscopy” by Eaton and West, OUP, 2010. The article comes from Chapter 3, which describes all of the commonly used modes in Atomic Force Microscopes. The Article in the book also contains a full reference list.

 


Images in this article come from the book, and are Copyright Peter Eaton/ OUP 2010.

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